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2 article(s) from Smykalla, Lars

Ester formation at the liquid–solid interface

Nguyen T. N. Ha,
Thiruvancheril G. Gopakumar,
Nguyen D. C. Yen,
Carola Mende,
Lars Smykalla,
Maik Schlesinger,
Roy Buschbeck,
Tobias Rüffer,
Heinrich Lang,
Michael Mehring and
Michael Hietschold

Beilstein J. Nanotechnol. 2017, 8, 2139–2150, doi:10.3762/bjnano.8.213

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Figure 1: Molecular structures of the molecules involved in the study and shortened forms of their names (in ...

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Figure 2: a) STM constant height image (1.2 V, 1 nA) of a TMA–undecanol linear pattern (LP0) formed on HOPG (...

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Figure 3: STM constant height image (1.2 V, 1 nA) of linear pattern LP4 (a), monoester type-I (c), and monoes...

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Figure 4: STM constant current image (1.1 V, 1 nA) of TMA–monoundecyl ester type-I obtained from a TMA–undeca...

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Figure 5: STM constant height images (1.2 V, 1.3 nA) of monoester obtained from a TMA–undecanol solution on H...

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Figure 6: Simulation of the STM constant height mode images (HOMO (a) and LUMO (b)) of a single monoester mol...

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Figure 7: STM constant height image (1.2 V, 1 nA) of the linear pattern of the synthesized monoester at the H...

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Scheme 1: Proposed scheme of ester formation from TMA and undecanol via an intermediate dimer.

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Figure 8: Energy diagram of the reaction path of TMA and undecanol to form TMA–undecyl ester and water for is...

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Figure 9: Three possible hypotheses for the formation of the monoester from TMA and undecanol.

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Supp Info

Full Research Paper

Published 12 Oct 2017

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(Metallo)porphyrins for potential materials science applications

Lars Smykalla,
Carola Mende,
Michael Fronk,
Pablo F. Siles,
Michael Hietschold,
Georgeta Salvan,
Dietrich R. T. Zahn,
Oliver G. Schmidt,
Tobias Rüffer and
Heinrich Lang

Beilstein J. Nanotechnol. 2017, 8, 1786–1800, doi:10.3762/bjnano.8.180

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Scheme 1: Chemical structures of (metallo)porphyrins under review here.

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Figure 1: Surface topography determined by AFM as a function of thickness. Cu-TMPP (= CuTPP(OMe)₄) (a) 35 nm,...

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Figure 2: Formation of molecular dendrites in a 117 nm thick Cu-TMPP (= CuTPP(OMe)₄) sample at different regi...

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Figure 3: Transport in Cu-TMPP (= CuTPP(OMe)₄) films and dendrites, (a–d) AFM topography characteristics. The...

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Figure 4: Extinction coefficient k for a) H₂TMPP, b) CuTMPP and c) NiTMPP. The uniaxial anisotropic model res...

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Figure 5: Energy dispersion of the magneto-optical Voigt constant Q for a) H₂TMPP, b) CuTMPP and c) NiTMPP. F...

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Figure 6: MCD (η_F) spectra in the Q-band region for a) H₂TMPP, b) CuTMPP and c) NiTMPP and the modelling with...

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Figure 7: Results of STM measurements: (a,b) Formation of small islands at submonolayer coverage. Molecules o...

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Figure 8: Highly resolved filled (a) and empty molecular states (b) STM image of the square structure of H₂TH...

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Figure 9: (a) Large scale STM image of submonolayer coverage showing molecular chains and ordered islands of H...

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Figure 10: (a–e) Manipulation of the electronic structure by applying a voltage pulse with the STM tip at the ...

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Figure 11: Left: Evolution of the XPS spectra of Br 3d for a molecular monolayer of CuTPP(Br)₈ on Au(111) as a...

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Figure 12: Results of STM measurements: (a) Novel structure of the alternating molecular rows formed after ann...

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Review

Published 29 Aug 2017

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